Mould and process optimisation

You have to be able to deal with pressure

When it comes to applying ultra-thin layers to surfaces such as screens, solar cells or semiconductors, there is no getting around the process of sputtering. In this process, a block of material – called a sputtering target – is bombarded with high-energy ions in a vacuum chamber. This releases tiny particles that are then deposited on the surface of the object to be coated. Metals (e.g. aluminium or copper), ceramics or an alloy can be used as the material. Read here how our Graphite People were able to help produce pressure-resistant sintering molds for the manufacture of sputtering targets and thus significantly optimize the processes.

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Background

Without the use of ultra-thin layers, most modern technologies would not be possible.

For example Touchscreens on displays only work because transparent, conductive layers are applied to the glass. With solar cells special coatings ensure that light can be efficiently converted into electricity and are also used in the manufacture of microprocessors and memory chips. microprocessors and memory chips the semiconductors are finely coated.

The production of sputtering targets is a technically high-precision process.

The starting material often consists of a mixture of different powders that are required for the final properties of the target. The powder is filled into an electrically conductive mold (e.g. square plate) and compacted under uniaxial pressure and temperature (Joule heat due to electrical energy). The powder is thus sintered into a solid, in this case a plate, and solidified.

Overview

Industry:

Tool, mold and machine construction

Procedure:

Pressure Sintering

(Field-Assisted Sintering Technique/ Spark Plasma Sintering)

Services:

Analysis and simulation, new design, production of sintered moulds

Result:

Increased process stability, quality and reliability as well as output per oven run

The challenge

When it comes to the mechanical stability of the targets, the high thermal and mechanical high thermal and mechanical loads on the mold pose a particular challenge. The mold may crack or warp. For this reason, the powder form should be designed to absorb induced mechanical and thermal stresses without cracking (multiple use). Likewise, no powder, which is entirely required for the output of the targets, should be lost as a result of the pressing via gaps, which are required for the demoldability of the target from the mold.

In addition, the raw materials used are extremely expensive and disruptions or interruptions to the process represent a high cost factor.

Process reliability and optimisation, durability and sustainability in recycling at the end of the life cycle are further key challenges.

The specific task: Optimisation of a sintering mould

In the example discussed here, the previous sintering mould could not withstand the pressure caused by the uniaxial pressing – it burst during the furnace run.

The following targets were set for optimisation:

  • Pressure-resistant sinter mould
  • Process stability
  • Maintain the mass and volume of the mould as far as possible
  • Increased process quality through optimised temperature consistency
  • Increased output per oven run thanks to maximised filling volume
  • Prevention of downtimes
Graphite Materials - Case studies - Sputtering - Sintering mold overloaded

Sintering mold overloaded

Graphite Materials - Case studies - Sputtering - Graphite mold

Process results

Based on the data supplied by the customer and the specified framework conditions such as temperature and pressure, we carried out an FEM simulation was carried out. We found that changing the inner corner radii was the best option for improving the shape.

Stable sintered mould

The proposed changes meant that there were no more cracks in the mould and therefore no interruptions in the production process.

Maintain the mass of the sintering mould

The optimisation was achieved without increasing the mass of the mould.

This made the change cost-efficient and effective.

Graphite Materials - Case studies - Sputtering - Sintering shape optimized

Sintering form optimized

The result

By changing the inner radius, the stresses in the mould could be reduced by 50 %.

The optimization of the mould contour led to a safe and stable process with multiple use of the mould. The material output of the targets was increased by optimizing the gap dimensions, thus increasing the added value.

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